The information is in this thread.
1. Connect your CF card, open Terminal and type "diskutil list". Take a look at which disk looks like your CF card (probably "/dev/disk1").
2. Open the FS-UAE config file (/Documents/FS-UAE/Configurations/Default.fs-uae) and add the line "hard_drive_0 = /dev/disk1" (or disk2 or whatever your CF card was)
I had a problem where my CF wasn't showing up at all in diskutil - but that was because my CF adapter was defective (cheap Chinese junk!). When you connect your CF, if you don't see the OSX "Disk Insertion" popup complaining that it was unreadable, then it probably wasn't detected.
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